Канал: WSU Chemistry 410

Experiment 12, Synthesis of Me5CpIrCl2 Dimer

Experiment 12, Synthesis of Me5CpIrCl2 Dimer

Using a McLeod Gauge to Measure Vacuum Pressure

Using a McLeod Gauge to Measure Vacuum Pressure

Using Rubberbands in Schlenk Line Manipulations

Using Rubberbands in Schlenk Line Manipulations

Removing Solvent on a Schlenk Line

Removing Solvent on a Schlenk Line

Experiment #11 Synthesis of KBArF4, Cp2FeBArF4, and AgBArF4

Experiment #11 Synthesis of KBArF4, Cp2FeBArF4, and AgBArF4

Experiment #6, Synthesis of 8-SMe-BODIPY

Experiment #6, Synthesis of 8-SMe-BODIPY

Vacuum Distillation

Vacuum Distillation

Air/Moisture Sensitive Filtrations

Air/Moisture Sensitive Filtrations

Preparation of an NMR Sample

Preparation of an NMR Sample

Experiment #1, Glow Sticks

Experiment #1, Glow Sticks

COVID-19 Disinfection Procedure

COVID-19 Disinfection Procedure

Experiment #2, Silicone Polymers

Experiment #2, Silicone Polymers

Experiment #7, Thermochromic Compounds

Experiment #7, Thermochromic Compounds

Experiment #3, Synthesis of Mn(acac)3

Experiment #3, Synthesis of Mn(acac)3

Operation of 500 MHz Varian NMR Spectrometer

Operation of 500 MHz Varian NMR Spectrometer

Experiment #8, Synthesis and Decomposition of tBuNH2BH3

Experiment #8, Synthesis and Decomposition of tBuNH2BH3

Greasing and Degreasing Ground Glass Joints

Greasing and Degreasing Ground Glass Joints

Experiment #4, Synthesis of (η6-Mesitylene)Mo(CO)3

Experiment #4, Synthesis of (η6-Mesitylene)Mo(CO)3

Using a Rotary Evaporator

Using a Rotary Evaporator

Experiment #9, Sublimation of Ferrocene and Synthesis of Cp2FePF6

Experiment #9, Sublimation of Ferrocene and Synthesis of Cp2FePF6

Cooling Chemical Reactions

Cooling Chemical Reactions

Heating Chemical Reactions

Heating Chemical Reactions

Collecting Liquid Nitrogen from a Dewar/Lockset

Collecting Liquid Nitrogen from a Dewar/Lockset

Experiment #5, Synthesis and Reactivity of Vaska's Complex

Experiment #5, Synthesis and Reactivity of Vaska's Complex

Setting Up & Taking Down a Schlenk Line

Setting Up & Taking Down a Schlenk Line

Transferring Solvents & Reagents with a Syringe on a Schlenk Line

Transferring Solvents & Reagents with a Syringe on a Schlenk Line

Transferring Solvents & Reagents with a Cannula on a Schlenk Line

Transferring Solvents & Reagents with a Cannula on a Schlenk Line

Introduction to Schlenk Lines

Introduction to Schlenk Lines

Using the Glovebox Antechambers/Ports

Using the Glovebox Antechambers/Ports

Introduction to a Glovebox

Introduction to a Glovebox

Using a Glovebox

Using a Glovebox

Using Septa

Using Septa

Experiment #10, Synthesis and O2 Uptake of Cosalen YouTube Final

Experiment #10, Synthesis and O2 Uptake of Cosalen YouTube Final

Column Chromatography

Column Chromatography

Making a Solid State IR Sample with a KBr Press

Making a Solid State IR Sample with a KBr Press

Making a Solid State IR Sample with a Nujol Mull

Making a Solid State IR Sample with a Nujol Mull

Making a Solution State IR Sample

Making a Solution State IR Sample

Using the "Freeze, Pump, Thaw Method" to Degas a Solution; Followed by Vacuum Transfer of a Solvent

Using the "Freeze, Pump, Thaw Method" to Degas a Solution; Followed by Vacuum Transfer of a Solvent